AOAC 2023.18 Saccharin Analysis in Dairy Powders
The AOAC International Standard Method 2023.18 provides a robust and reliable protocol for the quantification of saccharin in dairy powders. This method is widely recognized as an industry standard, ensuring consistency and accuracy across various laboratories.
Saccharin, being a synthetic sweetener, plays a significant role in enhancing flavor profiles while maintaining a low-calorie content in food products. However, its presence must be controlled to meet regulatory requirements. This method is particularly important for quality managers, R&D engineers, and compliance officers who need precise measurements of saccharin levels.
The AOAC 2023.18 method employs high-performance liquid chromatography (HPLC) with UV detection after derivatization of the sample to ensure accurate quantification. Sample preparation involves thorough homogenization followed by extraction using an appropriate solvent, typically methanol or acetonitrile.
Sample analysis requires careful handling and precise instrumentation. The HPLC system must be calibrated regularly according to ISO 86601:2017 for accurate results. Additionally, the method includes a quality control step where spiked samples are analyzed alongside standard samples to validate the analytical procedure.
This method is widely used in various industries such as dairy processing, food manufacturing, and quality assurance. It ensures that products meet international standards set by organizations like ISO and FDA. Accurate saccharin content measurement helps manufacturers comply with regulations and maintain product integrity.
Scope and Methodology
The scope of AOAC 2023.18 encompasses the quantification of saccharin in dairy powders, including milk powders, whey powders, and other similar products. The methodology involves several key steps:
- Sampling: Representative samples are collected from production batches.
- Sample preparation: Samples undergo thorough homogenization followed by extraction using methanol or acetonitrile.
- Instrumentation: High-performance liquid chromatography (HPLC) with UV detection is used for quantification.
The method also includes a quality control step where spiked samples are analyzed alongside standard samples to validate the analytical procedure. This ensures that the results obtained are accurate and reliable, meeting international standards set by organizations like ISO and FDA.
Eurolab Advantages
At Eurolab, we offer comprehensive services for AOAC 2023.18 saccharin analysis in dairy powders, leveraging our expertise to ensure accurate and reliable results:
- Accurate Results: Our state-of-the-art HPLC systems are regularly calibrated according to ISO standards.
- Compliance Expertise: We stay updated on the latest regulatory requirements, ensuring that our analyses meet international standards.
- Dedicated Team: Our team of experts provides personalized support and ensures that your samples are handled with care.
International Acceptance and Recognition
The AOAC International Standard Method 2023.18 for saccharin analysis in dairy powders is widely accepted across the globe due to its robustness and reliability:
- ISO Compliance: The method adheres to ISO standards, ensuring consistency and accuracy.
- FDA Recognition: This method is recognized by the U.S. Food and Drug Administration for compliance testing.
- EU Approval: The European Union also recognizes this method for its reliability in quantifying saccharin.