EN 14132 Ochratoxin Analysis in Barley and Malt Feed
The presence of ochratoxins, particularly Ochratoxin A (OTA), is a critical concern for the food & feed industry. OTA can be produced by certain strains of Aspergillus fungi during the growth or storage phases of crops like barley and malt. This mycotoxin poses significant health risks to both humans and animals, including nephrotoxicity and carcinogenic effects.
According to ISO 14132, this standard provides a methodology for the analysis of ochratoxin A in barley and malt feed. This service ensures compliance with international standards, thereby safeguarding consumer health and meeting regulatory requirements.
The process involves several stages including sample preparation, extraction, cleanup, concentration, and finally, chromatographic separation and quantification using high-performance liquid chromatography (HPLC) coupled with fluorescence detection. The method is designed to achieve accurate results down to the lowest detectable limits specified by the standard.
Our laboratory adheres strictly to this protocol, ensuring precision and reliability in every test. We use state-of-the-art equipment such as Agilent 1260 Infinity HPLC systems equipped with fluorescence detectors for optimal performance. Our team of experts is trained specifically on these instruments to guarantee consistent results.
Compliance with EN 14132 is essential not only for regulatory purposes but also for maintaining brand reputation and consumer trust. By conducting thorough analysis, we help our clients ensure that their products meet the highest quality standards set by international authorities.
The importance of this service cannot be overstated, especially given its role in preventing contamination risks associated with ochratoxins. Regular testing is crucial to monitor feed safety throughout the supply chain and maintain product integrity.
| Sample Preparation | Extraction Method | Cleanup Technique | Concentration Procedure | Chromatographic Separation & Quantification |
|---|---|---|---|---|
| - Grinding the sample into fine powder - Weighing an appropriate amount of the powder for analysis |
- Solvent extraction using acetonitrile - Ultrasonication to enhance dissolution |
- Solid-phase extraction (SPE) cartridges - Elution with methanol |
- Evaporation under nitrogen stream - Reconstitution in a mobile phase |
- Injection of the sample onto an HPLC column - Detection using fluorescence detection |
The above table outlines typical steps involved in preparing and analyzing samples according to EN 14132. Each step is crucial for obtaining accurate results.
To summarize, our EN 14132 Ochratoxin Analysis service provides comprehensive testing services that help protect your brand from potential contamination issues. Our commitment to accuracy and precision ensures you receive reliable data which can guide decision-making processes within your organization.
Scope and Methodology
The scope of this service includes the analysis of ochratoxin A in barley and malt feed samples based on ISO 14132. This method involves several key steps:
- Sample preparation: Grind the sample into fine powder, then weigh an appropriate amount for analysis.
- Extraction: Use acetonitrile and perform ultrasonication to dissolve the sample efficiently.
- Cleanup: Employ solid-phase extraction (SPE) cartridges followed by elution with methanol.
- Concentration: Evaporate under a nitrogen stream before reconstituting in the mobile phase.
- Injection: Inject the concentrated sample onto an HPLC column for separation and quantification via fluorescence detection.
The entire process is designed to ensure precise measurement down to the lowest detectable limits. Compliance with these steps guarantees accurate results every time.
Our laboratory follows this exact methodology ensuring consistency across all analyses conducted under EN 14132. By adhering strictly to this protocol, we provide reliable and reproducible data that meet international standards.
Industry Applications
- Quality Assurance in Food & Feed Production
- Regulatory Compliance for Export Markets
- R&D Projects Focusing on Contaminant Detection
- Supply Chain Monitoring to Ensure Product Integrity
- Internal Audits and Assessments
- Patient Safety Measures in Pharmaceutical Manufacturing
- Consumer Protection Initiatives Across Various Sectors
These applications highlight the versatility of our EN 14132 Ochratoxin Analysis service across different industries. Whether you're a large corporation or an SME, this service plays a vital role in maintaining product safety and compliance with global regulations.
Eurolab Advantages
At Eurolab, we pride ourselves on offering unparalleled expertise and advanced technology to our customers. Here are some key advantages of choosing us for your EN 14132 Ochratoxin Analysis needs:
- State-of-the-art Equipment: Equipped with Agilent 1260 Infinity HPLC systems and fluorescence detectors.
- Trained Experts: Our team is highly skilled in operating these sophisticated instruments to ensure accurate results.
- Comprehensive Support: From sample preparation to final report generation, we cover all aspects of the analysis process.
- Strict Compliance: Adhering meticulously to EN 14132, ensuring reliability and accuracy in every test conducted.
- Prompt Turnaround Time: Efficiently processing samples while maintaining high standards ensures timely delivery of results.
- Confidentiality Assurance: Protecting client information and data integrity is paramount to us.
With these advantages, Eurolab stands out as a trusted partner for all your laboratory testing needs. Our goal is to provide you with the most accurate and reliable results possible.
